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By Jose Ingacio Cabezon

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Surf Sci Rep 59 (1–6):151–152 13. Hibbeler RC (2003) Mechanics of materials. Pearson Prentice-Hall, Singapore 24 1 Physical Principles of Scanning Probe Microscopy Imaging 14. Kibble TWB, Berkshire FH (2004) Classical mechanics. Imperial College Press, London 15. Garcia R, Perez R (2002) Dynamic atomic force microscopy methods. Surf Sci Rep 47:197–301 16. Paulo AS, Garcia R (2002) Unifying theory of tapping-mode atomic-force microscopy. Phys Rev B 66, 041406(R) 17. Cleveland JP, Anczykowski B, Schmid AE, Elings VB (1998) Energy dissipation in tapping-mode atomic force microscopy.

Particular problems with tape have been observed for measurements in liquid media (compare Sect. 3). Alternatively, different types of glue, including epoxy or cyanoacrylate-based glues, can be used. Care has to be taken to avoid sample contamination. In particular, cyanoacrylates must not be covered during curing as they outgas material that deposits on the sample if covered. 3 Choice of Operation Modes and Suitable Imaging Environments The choice of operation modes and, if applicable, suitable imaging environments depend on many factors, including the type of polymer system to be analyzed and the type of information that is required.

0 V). 0. 0 Hz). If all these parameters have been adjusted and the vertical deflection signals have been checked, we can start the scan by pressing the “engage” button. During the descent of the tip, we closely monitor both vertical and lateral deflection signals on the LCD panels. Some variation of these signals (flickering) due to interference effects is typically observed. Upon descent, the vertical deflection signal may change monotonically, in particular for soft cantilevers for decreasing tipÀsample separation distances close to physical contact.

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