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Conducting Polymer Micro-/Nano- Structures ... 29 Figure 3. SEM images of the PANI as-synthesized at different stage: (a) initial stage “A”. (b) middle-stage “C”. (c) final-stage “E”. (d) UV-visible spectra of the PANI assynthesized at the “A”, “C”, “E” stage; (e) FTIR spectra of the PANI as-synthesized at different stage of “A”, “C”, and “E” stage; (f) Dependence of the conductivity and the doping level for PANI nanotubes synthesized by STFM. In order to understand formation mechanism of the nanotubes prepared by STFM, polymerization process with time was measured.

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J. Polym. Science part A: Polym. Chem. 1999, 37, 1277. , Sun, D. Polym. Bull. 2008, 60, 1. , Konyushenko, E. , Ciric-Marjanovic, G. J. Phys. Chem. B 2006, 110, 9461. , Konyushenko, E. , Holler, P. Polymer 2006, 47, 8253. [52] Do Nascimento G. , Silva, C. H. , Izumi, C. M. , Temperini, M. L. A. Spectrochim. Acta Part A 2008, 71, 869. [53] Do Nascimento, G. , Silva, C. H. , Temperini, M. L. A. Polym. Degrad. Stab. 2008, 93, 291. , Ivaska, A. Electrochem. Commun. 2006, 8, 1563. [55] Do Nascimento, G.

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